laboratory assignment laboratory techniques answers

laboratory assignment laboratory techniques answers

Laboratory Techniques and Measurements

Hands-On Labs, Inc.

Version 42-0165-00-02

Lab Report Assistant

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    This document is not meant to be a substitute for a formal laboratory report. The Lab Report Assistant is nothing more than a summary of the questions for the experiment, diagrams (if necessary), and data tables that would be included in a formal lab report. The intent is to facilitate students’ writing of lab reports by providing this information in an editable file that can be sent to an instructor.

    Exercise 1: Length, Temperature, and Mass

    Data Table 1. Length Measurements.

    Object

    Length (cm)

    Length (mm)

    Length (m)

    CD or DVD

    18 cm

    180 mm

    0.18 m

    Key

    5 cm

    50 mm

    0.05 m

    Spoon

    21 cm

    210 mm

    0.21 m

    Fork

    15 cm

    150 mm

    0.15 m

    Data Table 2. Temperature Measurements.

    Water

    Temperature (°C)

    Temperature (°F)

    Temperature (K)

    Hot from tap

    34o C

    95o F

    308 K

    Boiling

    97°C

    209°F

    367.15 K

    Boiling for 5 minutes

    104°C

    218°F

    494 K

    Cold from tap

    16°C

    57°F

    287.15 K

    Ice water – 1 minute

    11°C

    49°F

    282.15

    Ice water – 5 minutes

    5°C

    41°F

    278.15 K

    Data Table 3. Mass Measurements.

    Object

    Estimated Mass (g)

    Actual Mass (g)

    Actual mass (kg)

    Pen or pencil

    7g

    9g

    0.009 kg

    3 Pennies

    7.5 g

    7.5g

    0.0075 kg

    1 Quarter

    4 g

    5.7g

    0.0057 kg

    2 Quarters, 3 Dimes

    15 g

    18.2g

    0.0182 kg

    4 Dimes, 5 Pennies

    20 g

    22.1 g

    0.0221 kg

    3 Quarters, 1 Dime, 5 Pennies

    30 g

    32.6

    0.0326 kg

    Key

    6.5 g

    7.4

    0.0074 kg

    Key, 1 Quarter, 4 Pennies

    19.6 g

    23.1

    0.0231 kg

    Questions

    A. Water has a boiling point of 100°C at sea level. What might have caused the water in this experiment not to reach a boiling point of 100°C?

    At sea level, water turns to boiling at 100°C. The higher the water above the sea level, the lower the boiling point will be due to the decreased amount of pressure. The boiling point will be higher than 100°C if the water is below sea level because of the increased pressure in the air.

    B. While heating two different samples of water at sea level, one boils at 102°C and one boils at 99.2 °C. Calculate the percent error for each sample from the theoretical 100.0°C.

    For the first sample, which boils at 102°C, the percent error is 2 percent. The percent error calculated for sample 2 which boils at 99.2 degrees Celsius, is – 0.8 percent.

    Exercise 2: Volume and Density

    Data Table 4. Liquid Measurements.

      

    Mass A

    Mass B

    Mass B – A

      

    Liquid

    Volume (mL)

    Graduated Cylinder (g)

    Graduated Cylinder with

    liquid (g)

    Liquid (g)

    Density g/mL

    % Error

    Water

    5.0 ml

    5.0 ml

    5.0 ml

    5.0 ml

    5.0 ml

    5.0 ml

    Isopropyl alcohol

    19.4 g

    19.4 g

    19.4 g

    19.4 g

    19.4 g

    19.4 g

    Data Table 5. Magnet – Measurement Method.

    Object:

    Mass (g)

    Length (cm)

    Width (cm)

    Height (cm)

    Volume (cm3)

    Density (g/cm3)

    Magnet

    4 g

    2.5 cm

    0.25 cm

    0.25 cm

    0.16 cm3

    25 g/cm3

    Data Table 6. Displacement Method.

    Object

    Mass (g)

    Initial volume of graduated cylinder (mL)

    Final volume of graduated cylinder (mL)

    Object Volume (mL)

    Density (g/mL)

    Magnet

    4 g

    8 ml

    10 ml

    2 ml

    2g/ml

    Metal bolt

    7.6 g

    8 ml

    12 ml

    4 ml

    1.9g/ml

    Data Table 7. Archimedes’ method.

    Object

    Mass (g)

    Mass of Displaced Water (g)

    Volume of Displaced Water (mL)

    Density (g/mL)

    Metal Bolt

    7.6 g

    117.5 g

    116.4 ml

    1.07g/ml

    Magnet

    4 g

    117.1 g

    116.4 ml

    1.04 g/ml

    Questions

    A. A rectangular object has an unknown height, length, and width of 3.6 cm, 4.21 c,m and 1.17 cm, respectively. What is the density (in grams per milliliter) of this substance if the mass is 21.3 g?

    ** 1 gram = 1 cm       3.6 x 4.21 x 1.17 = 17.7           21.3g / 17.7mL = 1.2 g/mL the density is 1.2 mLml

    A sample of gold (Au) has a mass of 26.15 g. If the theoretical density is 19.30 g/mL, what is the volume of the sample of gold?

    ** Volume = Mass/Density     Volume- 26.15 g /19.30 g/mL = 1.4 mL

    B. What will happen if you drop the object in the beaker rather than submerge the object when using Archimedes’ Principle method?

    If you had dropped an object into the beaker rather than submerging the object, then the results that you obtained would have been If you had dropped an object into the beaker without the object being completely submerged, the results you obtained would have been could get the same as the volume of the object instead of the result based on the buoyancy.

    C.What is the difference in the density measurement of the magnet done by Archimedes’ principle compared with the density measurement done by the calculated volume? Which procedure would be more reliable? Why?

    Exercise 3: Concentration, Solution, and Dilution

    Data Table 8. Initial Concentration.

    Chemical

    Mass of

    Volumetric Flask

    Mass of Sugar (g)

    Molar Mass (g)

    Moles in Volumetric Flask

    Total Volume (L)

    Molarity (mol/L)

    Sugar (C12H22O11)

    27.3

    8

    342.296 g

    0.079755

    0.025

    3.1902

    mol/L

    Data Table 9. Dilution Series.

    Dilution

    Volume (mL)

    Mass (g)

    Density (g/mL)

    Initial Concentration (M)

    Volume Transferred (mL)

    Final Concentration (M)

    0

    25.0 mL

    27.7g

    1.108g/mL

     

    0 mL

    3.1902 M

    1

    25.0 mL

    24.9g

    0.996g/mL

    3.1902 M

    2.5 mL

    0.31902 M

    2

    25.0 mL

    25.4g

    0.984g/mL

    3.1902 M

    4.5 mL

    1.741444 M

    3

    25.0 mL

    25.1

    1.004g/mL

    3.1902 M

    3.0 mL

    2.612166 M

    4

    25.0 mL

    25.6

    1.024g/mL

    3.1902 M

    6.0 mL

    1.306083 M

    Data Table 10. Molarity vs. Density.

    Molarity vs. Density

    Questions

    From the graph of Molarity vs. Density, (made in Data Table 10), what was the relationship between the molarity of the sugar solution and the density of the sugar solution? **As the sugar solution density decreased, the molarity decreased. It was also true that the opposite was true.

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